4''-CHLORO-2''-FLUOROACETOPHENONE synthesis
- Product Name:4''-CHLORO-2''-FLUOROACETOPHENONE
- CAS Number:175711-83-8
- Molecular formula:C8H6ClFO
- Molecular Weight:172.58
372-19-0
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175711-83-8
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$8.00/1g
Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: 2 h / 105 °C
2.1: aluminum (III) chloride / carbon disulfide / 0.5 h / 0 - 20 °C
2.2: 48 h / 0 °C / Reflux
3.1: hydrogenchloride / methanol; water / 4 h / Reflux
4.1: hydrogenchloride; sodium nitrite / water / 0.25 h / -5 - 5 °C
4.2: 1 h / 25 °C
References:
Suzhou Jingye Pharmaceutical And Chemical Co., Ltd.;Shen Jianwei;Wu Heming CN110668948, 2020, A
198967-23-6
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75-16-1
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175711-83-8
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$8.00/1g
351-28-0
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175711-83-8
162 suppliers
$8.00/1g