4-CHLORO-7-TRIFLUORO METHOXYQUINOLINE synthesis
- Product Name:4-CHLORO-7-TRIFLUORO METHOXYQUINOLINE
- CAS Number:40516-31-2
- Molecular formula:C10H5ClF3NO
- Molecular Weight:247.6
1535-73-5
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: ethanol / 4 h / 70 °C
2: diphenylether / 0.8 h / 260 °C
3: lithium hydroxide monohydrate; sodium hydroxide / 6 h / 100 °C
4: diphenylether / 0.8 h / 260 °C
5: trichlorophosphate / 1 h / 120 °C
References:
Zhang, Chao;Tang, Yun-Sang;Meng, Chu-Ren;Xu, Jing;Zhang, De-Liang;Wang, Jian;Huang, Er-Fang;Shaw, Pang-Chui;Hu, Chun [International Journal of Molecular Sciences,2022,vol. 23,# 11,art. no. 6307]