4-ETHOXY-3-METHOXYBENZONITRILE synthesis
- Product Name:4-ETHOXY-3-METHOXYBENZONITRILE
- CAS Number:81259-56-5
- Molecular formula:C10H11NO2
- Molecular Weight:177.2
Yield:81259-56-5 100%
Reaction Conditions:
Stage #1: 3-methoxy-4-hydroxybenzonitrilewith sodium hydride in N,N-dimethyl-formamide at 0; for 0.583333 h;
Stage #2: ethyl bromide in N,N-dimethyl-formamide at 0 - 20;
References:
Ma, Anqi;Yu, Wenyu;Xiong, Yan;Butler, Kyle V.;Brown, Peter J.;Jin, Jian [MedChemComm,2014,vol. 5,# 12,p. 1892 - 1898] Location in patent:supporting information
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