4'-OCTYLOXYACETOPHENONE synthesis
- Product Name:4'-OCTYLOXYACETOPHENONE
- CAS Number:37062-63-8
- Molecular formula:C16H24O2
- Molecular Weight:248.36
111-83-1
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99-93-4
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37062-63-8
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$712.00/1G
Yield:37062-63-8 99%
Reaction Conditions:
with potassium carbonate in N,N-dimethyl-formamide at 80; for 24 h;
Steps:
2 Synthesis of Compound 1
Take a clean two bottle, add magnet,1.36 g of p-hydroxyacetophenone (about 10 mmol),9.66 g of bromooctane (about 50 mmol),6.91 g of potassium carbonate and 40 ml of anhydrous N,N-dimethylformamide solution.Under magnetic stirring, react at 80°C for 24 h.After the reaction was completed, water/methylene chloride was extracted several times and the organic phases were combined.After separation by a chromatography column, 2.46 g of light yellow liquid was obtained (approximately 99% yield).
References:
CN107501313,2017,A Location in patent:Paragraph 0049; 0051; 0052
1818-07-1
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75-36-5
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37062-63-8
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1818-07-1
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108-24-7
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$14.00/250ML
37062-63-8
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108-95-2
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$14.00/25g
37062-63-8
24 suppliers
$712.00/1G