4-tert-Butylcyclohexanol synthesis
- Product Name:4-tert-Butylcyclohexanol
- CAS Number:98-52-2
- Molecular formula:C10H20O
- Molecular Weight:156.27
98-54-4
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98-52-2
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Yield:98-52-2 99.9%
Reaction Conditions:
with hydrogen in tetrahydrofuran at 180; under 195020 Torr;
Steps:
1 Example 1
Example 1 A 50 wt.-% strength solution of p-tert-butylphenol was prepared in THF. Then 2500 g/h of this solution were passed with hydrogen at a temperature of 180° C. and an overall pressure of 2.6·107 Pa through a flow reactor, which was packed with 3.2 l of the Ru catalyst described above. Following removal of the solvent, by distillation, the hydrogenation product had the following composition: 99.9% of cis,trans-4-tert-butylcyclohexanol <0.01% of p-tert-butylphenol.
References:
BASF Aktiengesellschaft US6388149, 2002, B2 Location in patent:Page column 17
![2H-Pyran, 2-[[4-(1,1-dimethylethyl)cyclohexyl]oxy]tetrahydro-](/CAS/20180601/GIF/80356-16-7.gif)
80356-16-7
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98-52-2
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98-53-3
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98-52-2
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75-65-0
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108-95-2
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98-52-2
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13491-79-7
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74052-93-0
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98-52-2
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