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ChemicalBook CAS DataBase List 5-Methyl-4-nitroindole
61149-54-0

5-Methyl-4-nitroindole synthesis

1synthesis methods
4769-97-5 Synthesis
4-Nitroindole

4769-97-5
353 suppliers
$6.00/250mg

10553-07-8 Synthesis
1H-Indole, 7-Methyl-4-nitro-

10553-07-8
4 suppliers
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Yield:-

Reaction Conditions:

Stage #1: 4-nitro-1H-indoIe;methylmagnesium chloridewith N,N,N,N,N,N-hexamethylphosphoric triamide in tetrahydrofuran at -30; for 0.25 h;
Stage #2: with lead(IV) acetate;acetic acid in tetrahydrofuran;dichloromethane at -30 - 20;Title compound not separated from byproducts;

References:

Lu, Haige;He, Kaizhang;Kool, Eric T. [Angewandte Chemie - International Edition,2004,vol. 43,# 43,p. 5834 - 5836]

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