3-(3,5-DIMETHOXY-PHENYL)-3-OXO-PROPIONIC ACID METHYL ESTER synthesis
- Product Name:3-(3,5-DIMETHOXY-PHENYL)-3-OXO-PROPIONIC ACID METHYL ESTER
- CAS Number:677326-64-6
- Molecular formula:C12H14O5
- Molecular Weight:238.24
79-20-9
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Yield:677326-64-6 88%
Reaction Conditions:
Stage #1: acetic acid methyl esterwith lithium hexamethyldisilazane in tetrahydrofuran at -78; for 0.75 h;Inert atmosphere;
Stage #2: 3,5-dimethoxybenzoyl chloride in tetrahydrofuran at -78; for 0.5 h;Inert atmosphere;
References:
Sandridge, Matthew J.;France, Stefan [Organic Letters,2016,vol. 18,# 17,p. 4218 - 4221] Location in patent:supporting information
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