ChemicalBook CAS DataBase List DIETHYL 2-(4-CHLOROPHENYL)-1,1-CYCLOPROPANEDICARBOXYLATE

DIETHYL 2-(4-CHLOROPHENYL)-1,1-CYCLOPROPANEDICARBOXYLATE synthesis

6synthesis methods

Product Name:DIETHYL 2-(4-CHLOROPHENYL)-1,1-CYCLOPROPANEDICARBOXYLATE
CAS Number:74444-83-0
Molecular formula:C15H17ClO4
Molecular Weight:296.75

6827-40-3 Synthesis

[(4-Chlorophenyl)methylene]malonic acid diethyl ester

6827-40-3
12 suppliers
$646.84/1g

1774-47-6 Synthesis

1774-47-6
563 suppliers
$6.00/25g

DIETHYL 2-(4-CHLOROPHENYL)-1,1-CYCLOPROPANEDICARBOXYLATE

74444-83-0
26 suppliers
$325.00/1g

Yield:74444-83-0 96%

Reaction Conditions:

Stage #1: trimethylsulfoxonium iodidewith sodium hydride in dimethyl sulfoxide;mineral oil;Inert atmosphere;
Stage #2: diethyl 4-chlorobenzylidenemalonate in dimethyl sulfoxide;mineral oil at 15 - 60;Inert atmosphere;

References:

He, Xianran;Qiu, Guanpeng;Yang, Jin;Xiao, Yuling;Wu, Zhongyuan;Qiu, Guofu;Hu, Xianming [European Journal of Medicinal Chemistry,2010,vol. 45,# 9,p. 3818 - 3830] Location in patent:experimental part

1073-67-2 Synthesis

1073-67-2
310 suppliers
$7.00/5g

685-87-0 Synthesis

685-87-0
269 suppliers
$10.00/5g

74444-83-0
26 suppliers
$325.00/1g

References

1073-67-2 Synthesis

1073-67-2
310 suppliers
$7.00/5g

631-22-1 Synthesis

631-22-1
81 suppliers
$20.48/5g

74444-83-0
26 suppliers
$325.00/1g

References

105-53-3
811 suppliers
$5.00/25g

74444-83-0
26 suppliers
$325.00/1g

References

104-88-1 Synthesis

104-88-1
666 suppliers
$5.00/25g

74444-83-0
26 suppliers
$325.00/1g

References

DIETHYL 2-(4-CHLOROPHENYL)-1,1-CYCLOPROPANEDICARBOXYLATE Related Search:

DIETHYL 2-(PHENYLETHYL)MALONOATE ETHYL 1-METHYLCYCLOPROPANE-1-CARBOXYLATE 1,1-Cyclopropanedicarboxylic acid 1-METHYLCYCLOPROPANE-1-CARBOXYLIC ACID 1-HYDROXYMETHYL-CYCLOPROPANECARBOXYLIC ACID ETHYL ESTER LABOTEST-BB LT00408946 2-PHENYL-CYCLOPROPANECARBOXYLIC ACID 1,1-Cyclopropanedicarboxylic acid monomethyl ester 1,1-Bis(hydroxymethyl)cyclopropane

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DIETHYL 2-(4-CHLOROPHENYL)-1,1-CYCLOPROPANEDICARBOXYLATE synthesis

DIETHYL 2-(4-CHLOROPHENYL)-1,1-CYCLOPROPANEDICARBOXYLATE Related Search: