1,2,3,4-tetrahydro-isoquinoline-3-carboxylic acid methyl ester synthesis
- Product Name:1,2,3,4-tetrahydro-isoquinoline-3-carboxylic acid methyl ester
- CAS Number:79815-19-3
- Molecular formula:C11H13NO2
- Molecular Weight:191.23
252008-94-9
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79815-19-3
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Yield:79815-19-3 100%
Reaction Conditions:
Stage #1: methyl (3S)-2-(tert-butoxycarbonyl)-1,2,3,4-tetrahydro-3-isoquinolinecarboxylatewith trifluoroacetic acid in dichloromethane at 20; for 1 h;
Stage #2: with N-ethyl-N,N-diisopropylamine in dichloromethane at 20; for 0.25 h;
References:
Charton, Julie;Delarue, Sandrine;Vendeville, Sandrine;Debreu-Fontaine, Marie-Ange;Girault-Mizzi, Sophie;Sergheraert, Christian [Tetrahedron Letters,2001,vol. 42,# 43,p. 7559 - 7561]
63-91-2
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79815-19-3
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200644-47-9
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79815-19-3
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