N-[(4-chlorophenyl)methyl]-N',N'-diethylethane-1,2-diamine synthesis
2synthesis methods
- Product Name:N-[(4-chlorophenyl)methyl]-N',N'-diethylethane-1,2-diamine
- CAS Number:84434-83-3
- Molecular formula:C13H21ClN2
- Molecular Weight:240.77
Yield:-
Reaction Conditions:
with triethylamine in dichloromethane at 20; for 5 h;
Steps:
3.9
4-Chlorobenzylamine (1.0 mL, 8.2 mmol) was added to a solution of 2- brorno-N,N-diethylethylamine hydrobromide (2.4 g,9.0 mmol) and triethylamine (3.4 mL, 25 mmol) in dichloromethane (16 mL). The mixture was stirred at room temperature for 5 hours. The mixture was then concentrated to give Nl-(4-chlorobenzyl)-N2,N2-diethylethane-l,2- diamine as an oil which was used immediately without purification.
References:
WO2009/6569,2009,A1 Location in patent:Page/Page column 45
