3-Methoxy-α-[(triMethylsilyl)oxy]-benzeneacetonitrile synthesis
- Product Name:3-Methoxy-α-[(triMethylsilyl)oxy]-benzeneacetonitrile
- CAS Number:93554-98-4
- Molecular formula:C12H17NO2Si
- Molecular Weight:235.36
Yield:93554-98-4 99%
Reaction Conditions:
Stage #1: 3-methoxy-benzaldehydewith scandium tris(trifluoromethanesulfonate);1-n-butyl-3-methylimidazolium hexafluoroantimonate at 20; for 0.166667 h;
Stage #2: trimethylsilyl cyanide at 20; for 0.0833333 h;Inert atmosphere;
References:
Park, Boyoung Y.;Ryu, Ka Yeon;Park, Jung Hwan;Lee, Sang-Gi [Green Chemistry,2009,vol. 11,# 7,p. 946 - 948] Location in patent:experimental part
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