Methyl 4-((5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)carbamoyl)benzoate synthesis
- Product Name:Methyl 4-((5,5,8,8-tetramethyl-5,6,7,8-tetrahydronaphthalen-2-yl)carbamoyl)benzoate
- CAS Number:94497-53-7
- Molecular formula:C23H27NO3
- Molecular Weight:365.47
110-03-2
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Yield:-
Steps:
Multi-step reaction with 5 steps
1: conc. HCl, HCl gas / 0.25 h / 0 °C
2: 81.9 percent / AlCl3 / 24 h / Heating
3: 49.9 percent / HNO3, H2SO4 / 1 h / -10 °C
4: 48 percent / hydrogen / Pd/C / ethanol
5: 86.7 percent / pyridine / benzene / Ambient temperature
References:
Kagechika, Hiroyuki;Kawachi, Emiko;Hashimoto, Yuichi;Himi, Toshiyuki;Shudo, Koichi [Journal of Medicinal Chemistry,1988,vol. 31,# 11,p. 2182 - 2192]
92050-16-3
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7377-26-6
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6223-78-5
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6683-46-1
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