ChemicalBook CAS DataBase List ALLYL PHENYL SULFOXIDE

ALLYL PHENYL SULFOXIDE synthesis

12synthesis methods

Product Name:ALLYL PHENYL SULFOXIDE
CAS Number:19093-37-9
Molecular formula:C9H10OS
Molecular Weight:166.24

Oxidation of Allyl Phenyl Sulfide in dichloromethane with m-Chloroperbenzoic Acid acid (1.2 equiv) added slowly as a solution in dichloromethane at -70 °C affords the sulfoxide in high yields with minimal over-oxidation to the sulfone. The m-chlorobenzoic acid formed may be removed simply by filtration. Other oxidizing agents such as Sodium Bromite3 and Trifluoroperacetic Acid4 afford the sulfoxide in yields greater than 80% and are also highly selective.

5296-64-0
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19093-37-9
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Yield:19093-37-9 100%

Reaction Conditions:

with 2-hydroperoxy-2-methoxypropane in methanol;

References:

Leriverend, Pierre;Leriverend, Marie-Louise [Synthesis,1987,# 6,p. 587 - 588]

5296-64-0
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16212-05-8 Synthesis

16212-05-8
147 suppliers
$14.00/250mg

19093-37-9
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References

6099-23-6
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106-95-6 Synthesis

106-95-6
423 suppliers
$10.00/5g

19093-37-9
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References

133670-27-6 Synthesis

Benzenesulfinothioic acid, S-phenyl ester, (-)- (9CI)

133670-27-6
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2622-05-1 Synthesis

2622-05-1
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$40.00/500mg

5296-64-0
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19093-37-9
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References

Benzenesulfinic acid, 2-propen-1-yl ester

92838-57-8
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19093-37-9
17 suppliers
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References

ALLYL PHENYL SULFOXIDE Related Search:

Allyl phenyl sulfone Phenyl sulfoxide DIOXO(PHENYL)(3-PHENYL-2-PROPENYL)-LAMBDA6-SULFANE

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ALLYL PHENYL SULFOXIDE synthesis

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