Anthracene synthesis
- Product Name:Anthracene
- CAS Number:120-12-7
- Molecular formula:C14H10
- Molecular Weight:178.23
100622-34-2
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120-12-7
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Yield:120-12-7 91%
Reaction Conditions:
with sodium hypochlorite;tetrabutylammomium bromide;water at 100;
Steps:
Protodeboronation of Arylboronic Acids; General Procedure
General procedure: A solution of the appropriate arylboronic acid (1 mmol) andTBAB (64 mg, 0.2 mmol) in 10.5 wt% aq NaClO was stirred at100 °C for 6-12 h until the reaction was complete (TLC). Themixture was extracted with Et2O (2 × 5 mL), and the organiclayer was dried (Na2SO4) and concentrated in vacuo. The residuewas purified by column chromatography [silica gel, PE-EtOAc(40:1 to 20:1)].
References:
Li, Minxin;Tang, Yanling;Gao, Jinchun;Rao, Gaoxiong;Mao, Zewei [Synlett,2020,vol. 31,# 20,p. 2039 - 2042]
642-31-9
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120-12-7
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32832-95-4
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120-12-7
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1210-12-4
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120-12-7
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4985-70-0
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$165.00/1g
120-12-7
339 suppliers
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