Benzyl acetate synthesis
- Product Name:Benzyl acetate
- CAS Number:140-11-4
- Molecular formula:C9H10O2
- Molecular Weight:150.17
100-39-0
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$10.00/10g
140-11-4
685 suppliers
$6.00/25g
Yield:140-11-4 90%
Reaction Conditions:
with silver(I) acetate in acetonitrile at 50; for 4 h;Inert atmosphere;Darkness;
Steps:
General procedure for acetoxylation of alkyl halides with AgOAc.
General procedure: To a suspension of AgOAc (0.25 mmol) in MeCN or DMF (2 mL) was added the alkylhalide (0.25 mmol) dissolved in 1 mL of the corresponding solvent. The reaction mixture was stirred at the temperature indicated on table 1 until starting material was consumed. After that, a saturated solution of NH4Cl (20 mL) was added and the crude mixture was extracted three times with EtOAc (3 x 15 mL). When necessary, the product was purifiedby column chromatography (hexane/EtOAc).
References:
Nolla-Saltiel, Roberto;Carrillo-Arcos, Ulises Alonso;Porcel, Susana [Synthesis,2014,vol. 46,# 2,p. 165 - 169] Location in patent:supporting information
127-09-3
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100-39-0
431 suppliers
$10.00/10g
140-11-4
685 suppliers
$6.00/25g
2754-27-0
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$8.00/5g
100-51-6
1421 suppliers
$5.00/100g
140-11-4
685 suppliers
$6.00/25g
108-22-5
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$20.00/25mL
100-51-6
1421 suppliers
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140-11-4
685 suppliers
$6.00/25g
935-04-6
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$53.00/5g
140-11-4
685 suppliers
$6.00/25g