ChemicalBook CAS DataBase List Caronic anhydride

Caronic anhydride synthesis

8synthesis methods

Product Name:Caronic anhydride
CAS Number:67911-21-1
Molecular formula:C7H8O3
Molecular Weight:140.14

At present, the synthetic method of Caronic anhydride is mainly taking chrysanthemum monocarboxylate as raw material, after oxidation, saponification, acidifying and cyclodehydration, be prepared from.

3,3 DIMETHYL CIS 1,2 CYCLOPROPANE DICARBOXYLIC ACID

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67911-21-1
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Yield:67911-21-1 91.97%

Reaction Conditions:

with acetic anhydride at 120 - 160; for 7 h;

Steps:

1-6

General procedure: Add 50mL of acetic anhydride to the above solution containing caronic acid, under 120 °C conditions, the insulation reflux reaction for 3h, continue to heat up to 160 °C, and insulate reflux reaction for 4h. Subsequently, caronic anhydride was distilled under reduced pressure to 18.46 g with a yield of 87.83%.

References:

CN114539046,2022,A Location in patent:Paragraph 0097; 0099; 0100-0106

124-38-9
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497-42-7
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67911-21-1
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References

108-31-6 Synthesis

108-31-6
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$13.47/50g

1530-33-2
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$18.00/5g

67911-21-1
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References

Cyclopropanecarboxylic acid, 3-[(acetyloxy)methyl]-2,2-dimethyl-, ethyl ester

79942-64-6
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67911-21-1
322 suppliers
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References

924-50-5 Synthesis

924-50-5
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$23.00/5g

67911-21-1
322 suppliers
$6.00/1g

References

Caronic anhydride Related Search:

Triethyl phosphate ACETONE-D6 Maleic anhydride Phthalic anhydride Dimethyl sulfoxide Dimethyl carbonate Dimethyl ether Hexane Isatoic Anhydride

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Caronic anhydride synthesis

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