Cuprous iodide synthesis
- Product Name:Cuprous iodide
- CAS Number:7681-65-4
- Molecular formula:CuI
- Molecular Weight:190.45
1586771-53-0
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7681-65-4
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Yield:-
Reaction Conditions:
in methanol; for 0.25 h;Cooling with ice;
Steps:
2.2.2.3. Synthesis of [Cu(L)I] (6).
For the synthesis of this complex, asolution of CuNO3.5H2O (0.246 g, 1 mmol) in 10 mL of methanol and a solution of NaI (0.1525 g, 1 mmol) in 10 mL of methanol were mixed and boiled for 15 min and then chilled in ice. The precipitated CuI was filtered and CuI was treated with a solution of thiosemicarbazone, HL (0.284 g, 1 mmol) in 10 mL hot methanoland refluxed for 4 h and cooled. The dark green shining crystals formed were filtered, washed with few drops of methanol andether and dried over P4O10 in vacuo.
References:
Jayakumar;Sithambaresan;Aravindakshan, A. Ambili;Kurup, M.R. Prathapachandra [Polyhedron,2014,vol. 75,p. 50 - 56]
7758-99-8
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7681-11-0
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7681-65-4
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14362-44-8
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7681-65-4
588 suppliers
$6.00/5g
7758-99-8
585 suppliers
$6.00/25g
7681-65-4
588 suppliers
$6.00/5g