IODO(TRIETHYL PHOSPHITE)COPPER(I), 97% synthesis
1synthesis methods
- Product Name:IODO(TRIETHYL PHOSPHITE)COPPER(I), 97%
- CAS Number:51717-23-8
- Molecular formula:C6H15CuIO3P
- Molecular Weight:356.6057
Iodo(triethyl phosphite)copper(I) is synthesized in 88.6% yield by addition of Copper(I) Iodide to a solution of Triethyl Phosphite in benzene; the mixture is stirred and heated until the CuI dissolves; the complex is obtained upon evaporation of the solvent under reduced pressure.1
Yield:51717-23-8 69.8%
Reaction Conditions:
in toluene at 80; for 8 h;Inert atmosphere;
References:
Ziegler;Fowler;Rodgers;Wester [Organic Syntheses,1987,vol. 65,p. 108 - 108]