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ChemicalBook CAS DataBase List Cyclohexanemethanol
100-49-2

Cyclohexanemethanol synthesis

14synthesis methods
To 1 g benzyl alcohol in 40 ml of H20, HRO/Na- β catalyst (50 mg) was added in a reactor vessel. The reactor vessel was then heated at 100 °C for 1 h under H2 pressure (20 bar). After completion of the reaction, the catalyst was separated by using centrifuge and the obtained clear product mixture was analyzed by GC-MS. The reaction gave 100% conversion of benzyl alcohol with 100% yield of Cyclohexanemethanol.
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Yield:100-49-2 100%

Reaction Conditions:

with hydrogen in water at 100; under 15001.5 Torr; for 1 h;

Steps:

21 Example: 21

To 1 g benzyl alcohol in 40 ml of H20, HRO/Na- β catalyst (50 mg) was added in a reactor vessel. The reactor vessel was then heated at 100 °C for 1 h under H2 pressure (20 bar). After completion of the reaction, the catalyst was separated by using centrifuge and the obtained clear product mixture was analyzed by GC-MS. The reaction gave 100% conversion of benzyl alcohol with 100% yield of cyclohexylmethanol.

References:

WO2017/60922,2017,A1 Location in patent:Page/Page column 15; 21; 22

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