Cyclohexyldimethoxymethylsilane synthesis
- Product Name:Cyclohexyldimethoxymethylsilane
- CAS Number:17865-32-6
- Molecular formula:C9H20O2Si
- Molecular Weight:188.34
16881-77-9
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$53.39/5g
110-83-8
329 suppliers
$11.00/25g
17865-32-6
193 suppliers
$6.00/25g
Yield:17865-32-6 65%
Reaction Conditions:
with C22H31N2O7Rh in neat (no solvent) at 25; for 12 h;Reagent/catalyst;Temperature;
Steps:
11 Examples 11 and 12
To a cyclohexene solution (0.5 mL) of Rh (Phebox-iPr) (OAc) 2 OH 2 (5.4 mg, 0.010 mmol) represented by the following formula,Hydrosilane (amount shown in Table 5) listed in Table 5 was added.After stirring at 25 ° C. for 12 hours,Pentadecane (42.5 mg, 55.2 μL, 0.20 mmol) was added and the yield of each product was determined by measuring GC. As a result, the product of Example 11 (n = 1) was obtained in a yield of 65% and the product of Example 12 (n = 0) in a yield of 72%.
References:
NATIONAL INSTITUTE OF ADVANCED INDUSTRIAL SCIENCE AND TECHNOLOGY;Hayashi, Kazufumi;Matsumoto, Kazuhiro;Nakajima, Yumiko;Shimada, Shigeru;Sato, Kazuhiko JP2018/118920, 2018, A Location in patent:Paragraph 0022; 0025; 0028; 0031; 0034; 0035; 0036
1634-04-4
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5578-42-7
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$45.00/5 g
17865-32-6
193 suppliers
$6.00/25g
1185-55-3
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931-51-1
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$42.00/100ml
17865-32-6
193 suppliers
$6.00/25g
108-85-0
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$5.00/10g
1185-55-3
493 suppliers
$6.00/25g
17865-32-6
193 suppliers
$6.00/25g