Diallylamine synthesis
- Product Name:Diallylamine
- CAS Number:124-02-7
- Molecular formula:C6H11N
- Molecular Weight:97.16
538-08-9
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$106.00/250mg
124-02-7
251 suppliers
$14.00/5mL
Yield:-
Reaction Conditions:
with sulfuric acid in water at 30;
Steps:
1.1.3; 1.1.4
(3) Dehydration section: The upper distillation component is collected and pumped into the dehydration kettle to cool down to below 30 °C, the stirring is started, and the quantitative solid alkali dehydration is added.Dehydrated oil phase water ≤ 1.5%, concentrated dehydration components to be rectified. (4) Refinement section: pumping the dehydrated component into the rectification vessel, atmospheric distillation,The pre-collection fraction was collected and the finished diallylamine was collected when the top temperature reached 112 °C. The prepared diallylamine is a colorless transparent liquid, and the color is measured by a colorimeter with a color of 18,The content of the gas was determined by GC gas chromatography to be 99.3%, and the water was measured by Karl Fischer method, and the water content was equal to 0.20%.
References:
CN109369413,2019,A Location in patent:Paragraph 0047; 0048; 0051; 0052; 0053
463-49-0
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102-70-5
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107-11-9
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$29.09/25ml
124-02-7
251 suppliers
$14.00/5mL
463-49-0
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107-11-9
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124-02-7
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$14.00/5mL
109-73-9
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$9.00/1g
107-18-6
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$24.60/100ml
4538-09-4
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124-02-7
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111-26-2
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107-18-6
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22774-71-6
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124-02-7
251 suppliers
$14.00/5mL