DICHLORPROP-METHYL ESTER synthesis
- Product Name:DICHLORPROP-METHYL ESTER
- CAS Number:57153-17-0
- Molecular formula:C10H10Cl2O3
- Molecular Weight:249.09
2065-24-9
23 suppliers
inquiry
57153-17-0
32 suppliers
$70.00/100mg
Yield:57153-17-0 249.77 g
Reaction Conditions:
with 2,4,5-tri-tert-butylisothiazole,;chlorine;magnesium chloride at -20; for 0.5 h;
Steps:
4.2
To the obtained methyl 2-phenoxypropionate,Add 1.21 g of 99% pure magnesium chloride and 0.28 g of purity 99%2,4,5-tri-tert-butylisothiazole,170.45 g of 99% pure chlorine gas was introduced at -20 ° C to react.After the addition, the reaction was kept at this temperature for 0.5 h.249.77 g of methyl 2-(2,4-dichlorophenoxy)propanoate was obtained in an amount of 98.40%.
References:
CN108947814,2018,A Location in patent:Paragraph 0090; 0092
5445-17-0
288 suppliers
$6.00/25g
120-83-2
406 suppliers
$12.90/100g
57153-17-0
32 suppliers
$70.00/100mg
67-56-1
792 suppliers
$9.00/25ml
120-36-5
144 suppliers
$10.00/500mg
57153-17-0
32 suppliers
$70.00/100mg
108-95-2
778 suppliers
$14.00/25g
57153-17-0
32 suppliers
$70.00/100mg
58048-37-6
10 suppliers
inquiry
57153-17-0
32 suppliers
$70.00/100mg