Diethylamine hydrochloride synthesis
- Product Name:Diethylamine hydrochloride
- CAS Number:660-68-4
- Molecular formula:C4H12ClN
- Molecular Weight:109.6
109-89-7
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660-68-4
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Yield:660-68-4 100%
Reaction Conditions:
with hydroxylamine hydrochloride in ethanol for 2 h;Reflux;
Steps:
General procedure for the preparation of amine hydrochloride salts 2c-2r
General procedure: To a 25-mL round-bottomed flask containing ammonium chloride (0.54 g, 10 mmol) was added ethanol (3 mL) followed by the requisite amine (10 mmol). The mixture was magnetically stirred and refluxed for 2 h. The solvent was then removed by rotary evaporation affording the hydrochloride salt as a solid invariably in quantitative yield.
References:
Di Grandi, Martin J.;Bennett, Caitlin;Cagino, Kristen;Muccini, Arnold;Suraci, Corey;Saba, Shahrokh [Synthetic Communications,2015,vol. 45,# 22,p. 2601 - 2607] Location in patent:supporting information
771-99-3
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24424-99-5
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660-68-4
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$14.00/25g
123387-49-5
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194149-25-2
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660-68-4
441 suppliers
$14.00/25g
74289-57-9
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