Triethylamine hydrochloride synthesis
- Product Name:Triethylamine hydrochloride
- CAS Number:554-68-7
- Molecular formula:C6H16ClN
- Molecular Weight:137.65
96-45-7
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554-68-7
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$6.00/25g
Yield:554-68-7 97%
Reaction Conditions:
with triethylamine in tetrahydrofuran;
Steps:
147.B B.
30.6 parts by weight of imidazolidine-2-thione were boiled overnight with 54.4 parts by weight of trimethylchlorosilane and 51.5 parts by weight of triethylamine in absolute tetrahydrofurane. The warm suspension was freed of the precipitated triethylamine hydrochloride by filtration, and the filtrate was evaporated and dried in a vacuum desiccator. Melting point: approx. 130°C; Yield: 97%. Calculated: N, 14.4; S, 16.5; Found: N, 13.8; S, 16.9.
References:
US3933795,1976,A
685-91-6
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554-68-7
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131933-37-4
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96-53-7
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492454-84-9
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554-68-7
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$6.00/25g
4856-97-7
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814-49-3
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1428649-67-5
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554-68-7
500 suppliers
$6.00/25g