Diglycolic acid synthesis
- Product Name:Diglycolic acid
- CAS Number:110-99-6
- Molecular formula:C4H6O5
- Molecular Weight:134.09
3041-16-5
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110-99-6
294 suppliers
$29.50/25g
Yield:110-99-6 75%
Reaction Conditions:
with dinitrogen tetraoxide in chloroform
Steps:
III EXAMPLE III
EXAMPLE III A reaction vessel fitted with a condenser, and an agitator is charged with a solution of 4 parts of dinitrogen tetraoxide in 250 parts of chloroform. Into the agitated solution, about 10 parts of p-dioxanone is slowly added while the temperature is kept below 30°C. In the next 24 hours, an additional 4 parts of dinitrogen tetraoxide is added, and the reaction is allowed to proceed for another 50 hours at 20°-30°C. The reaction mixture is then stripped off all nitrogen oxides by bubbling air through the system. Diglycolic acid is recovered by filtration at a yield of about 75%.
References:
Monsanto Company US3952054, 1976, A
50-00-0
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201230-82-2
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110-99-6
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79-14-1
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110-88-3
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201230-82-2
1 suppliers
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110-99-6
294 suppliers
$29.50/25g
79-14-1
850 suppliers
$6.00/25g
50-00-0
901 suppliers
$10.00/25g
201230-82-2
1 suppliers
inquiry
110-99-6
294 suppliers
$29.50/25g
64-18-6
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$22.12/250ML
79-14-1
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625-45-6
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