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ChemicalBook CAS DataBase List Dimethyl L-cystinate dihydrochloride
32854-09-4

Dimethyl L-cystinate dihydrochloride synthesis

2synthesis methods
Measure 150mL of anhydrous methanol in a 250mL round-bottomed flask, slowly add SOCl2 (8.0mL, 108mmol) dropwise, and then add 10g of L-cystine to the reaction solution in batches. After returning to room temperature, refluxed at 60°C for 5 h. At the end o
-

Yield:32854-09-4 100%

Reaction Conditions:

with chloro-trimethyl-silane

References:

Naini, Santhosh Reddy;Ranganathan, Subramania;Yadav, Jhillu Singh;Sarma;Ramakrishna;Nagaraj, Ramakrishnan;Premkumar, J. Richard;Sastry, G. Narahari [Tetrahedron Letters,2014,vol. 55,# 6,p. 1132 - 1135]

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