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ChemicalBook CAS DataBase List Dimethylamine hydrochloride
506-59-2

Dimethylamine hydrochloride synthesis

6synthesis methods
Dimethylamine hydrochloride is obtained from the salt formation of dimethylamine and hydrochloric acid.
-

Yield:506-59-2 3 g

Reaction Conditions:

with hydrogenchloride in water at 0; for 0.5 h;

Steps:



Me2NH.HCl was prepared from aq dimethylamine solution (5.0 mL, 40%) by theaddition of conc. HCl (5.0 mL, 35%) at 0 C. The reaction mixture was stirred for0.5 h and then the water was evaporated. The solid fraction was azeotropedthrice with toluene to afford white solid compound (3.0 g), which was storedunder inert atmospher

References:

Khatik, Gopal L.;Sharma, Ratnesh;Kumar, Varun;Chouhan, Mangilal;Nair, Vipin A. [Tetrahedron Letters,2013,vol. 54,# 45,p. 5991 - 5993]

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