Dodecaethylene glycol monomethyl ether synthesis
- Product Name:Dodecaethylene glycol monomethyl ether
- CAS Number:5702-16-9
- Molecular formula:C25H52O13
- Molecular Weight:560.67
112-60-7
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5702-16-9
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Yield:-
Steps:
Multi-step reaction with 4 steps
1.1: triethylamine; dmap; thionyl chloride / dichloromethane / 0 - 25 °C
1.2: 0 - 25 °C
2.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h
2.2: 20 °C
2.3: 25 °C / pH 3
3.1: sodium hydride / tetrahydrofuran; mineral oil / 0.5 h / 0 °C / Inert atmosphere
3.2: 0 - 25 °C
4.1: palladium 10% on activated carbon; hydrogen / methanol / 12 h / 25 °C / 22502.3 Torr / Autoclave
References:
Xia, Guiquan;Li, Yu;Yang, Zhigang;Jiang, Zhong-Xing [Organic Process Research and Development,2015,vol. 19,# 11,p. 1769 - 1773]
23783-42-8
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5702-16-9
96 suppliers
$165.00/1 g
![2-[2-[2-[2-(BENZYLOXY)ETHOXY]ETHOXY]ETHOXY]ETHANOL](/CAS/GIF/86259-87-2.gif)
86259-87-2
148 suppliers
$24.00/1g
5702-16-9
96 suppliers
$165.00/1 g
477775-73-8
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5702-16-9
96 suppliers
$165.00/1 g