DODECYL ACETATE synthesis
- Product Name:DODECYL ACETATE
- CAS Number:112-66-3
- Molecular formula:C14H28O2
- Molecular Weight:228.37
108-22-5
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112-53-8
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112-66-3
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Yield:112-66-3 89%
Reaction Conditions:
with tetraethylammonium bicarbonate at 60; for 2 h;
Steps:
Typical procedure for transesterification of esters with alcohols (4aa as an example)
General procedure: In a typical procedure, in a capped vessel alcohol 3a (0.5 mmol) and ester 2a (1.5 mmol) were added sequentially to the TEAHC (35.0 mg, 0.15 mmol); the reaction mixture was stirred for 2 h at 60 °C and then transferred in a round-bottomed flask and concentrated under reduced pressure. The residue mixture was then extracted with diethyl ether (3 times with 10 cm3). After removal of the solvent from the combined ethereal layers under reduced pressure, the crude reaction mixture was analyzed by 1H and 13C NMR and thin-layer chromatography (TLC). All products were purified by using flash chromatography (n-hexane / ethyl acetate, 95/5) and identified on the basis of NMR spectroscopic analysis by comparison with reported data.
References:
Chiarotto, Isabella [Synthetic Communications,2016,vol. 46,# 22,p. 1840 - 1847] Location in patent:supporting information
112-53-8
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112-66-3
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112-53-8
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141-78-6
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112-66-3
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112-53-8
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64-19-7
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112-66-3
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39695-18-6
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141-78-6
748 suppliers
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112-66-3
169 suppliers
$21.00/25mL