ETHYL 2-ACETYL-3-OXO-HEXANOATE synthesis
- Product Name:ETHYL 2-ACETYL-3-OXO-HEXANOATE
- CAS Number:63765-76-4
- Molecular formula:C10H16O4
- Molecular Weight:200.23
Yield:63765-76-4 75%
Reaction Conditions:
Stage #1: ethyl acetoacetatewith pyridine;magnesium chloride in dichloromethane at 0; for 0.25 h;Inert atmosphere;
Stage #2: butyryl chloride in dichloromethane at 0 - 20; for 1.25 h;Inert atmosphere;
References:
Betard, Angelique;Wannapaiboon, Suttipong;Fischer, Roland A. [Chemical Communications,2012,vol. 48,# 85,p. 10493 - 10495,3] Location in patent:supporting information Betard, Angelique;Wannapaiboon, Suttipong;Fischer, Roland A. [Chemical Communications,2012,vol. 48,# 85,p. 10493 - 10495] Location in patent:supporting information
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