ETHYL N-PROPYL ETHER synthesis
- Product Name:ETHYL N-PROPYL ETHER
- CAS Number:628-32-0
- Molecular formula:C5H12O
- Molecular Weight:88.15
557-31-3
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628-32-0
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$90.00/2.5ml
Yield: 93%
Reaction Conditions:
with tetrakis[3,5-bis(trifluoromethyl)phenyl]boric acid bis(diethyl ether) complex;(bis[(2-dicyclohexylphosphino)ethyl]amine)cobalt(II)(CH2SiMe3);hydrogen in tetrahydrofuran at 50; under 760.051 Torr; for 24 h;
Steps:
General procedure: For three parallel reactions, complex 1(6.1mg, 10.0 tmol) and H[BAr’4](Et2O)2 (10.1 mg, 10.0 tmol) were dissolved in THF (2.0 mL) in a thick-walled glass vessel equipped with a Teflon stopcock and a stir bar. Acetophenone (60 mg, 0.5 mmol) was then added and hexamethylbenzene (0.1 mmol) was also added as internal standard. The reaction mixture was degassed by freeze-pump-thaw and charged with 1 atm (or 4 atm) of hydrogen gas. The resulting solution was stirred at 25° C. or 60° C. for 4 hours (see Equation 5), and then stopped in order to compare relative reaction rates.
References:
LOS ALAMOS NATIONAL SECURITY, LLC;Vasudevan, Kalyan V.;Zhang, Guoqi;Hanson, Susan K. US2015/336862, 2015, A1 Location in patent:Paragraph 0060; 0061
115-80-0
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4744-08-5
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628-32-0
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$90.00/2.5ml
557-31-3
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$49.00/5mL
998-30-1
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628-32-0
51 suppliers
$90.00/2.5ml
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
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628-32-0
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$90.00/2.5ml
71-23-8
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75-07-0
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$14.00/5mL
628-32-0
51 suppliers
$90.00/2.5ml