Ethyl 5-bromovalerate synthesis
- Product Name:Ethyl 5-bromovalerate
- CAS Number:14660-52-7
- Molecular formula:C7H13BrO2
- Molecular Weight:209.08
2067-33-6
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$6.00/5g
14660-52-7
250 suppliers
$6.00/5g
Yield:-
Reaction Conditions:
with thionyl chloride in ethanol
Steps:
14.A Di-[(5-N,N-dibutylamino)pentyl] carbonate dihydrochloride hydrate
A] Starting from 5-bromopentanoic acid (50 g, 0.276 mole) and thionyl chloride (39 ml, 0.552 mole) in absolute ethanol (500 ml) and following the procedure of Example 13,A], there were obtained 62.7 g of ethyl 5-bromopentanoate (quantitative yield) which was used as such in the next step.
References:
ITALFARMACO S.p.A. EP748310, 1999, B1
626-86-8
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14660-52-7
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5414-21-1
169 suppliers
$10.00/5g
14660-52-7
250 suppliers
$6.00/5g
