HEXACHLOROBENZENE synthesis
- Product Name:HEXACHLOROBENZENE
- CAS Number:118-74-1
- Molecular formula:C6Cl6
- Molecular Weight:284.78
Yield:-
Reaction Conditions:
under 0.01 Torr;Pyrolysis;
Steps:
FVP
General procedure: A flask (100 mL) containing the sample (100 mg) wasattached to an empty quartz tube (inner diameter 30 mm, length: 110 cm)placed in a horizontal tubular furnace (heated zone: 65 cm) and connected to acold trap (196 C). Pyrolysis was performed at 102 Torr, temperature: 300-1000 C. After the experiment, the cold trap was flushed with N2, warmed toambient temperature and the products were dissolved in chloroform andanalysed.
References:
Schollmeyer, Dieter;Detert, Heiner [Tetrahedron Letters,2017,vol. 58,# 9,p. 843 - 846] Location in patent:supporting information
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