HEXAETHYLDISILANE synthesis
- Product Name:HEXAETHYLDISILANE
- CAS Number:1633-09-6
- Molecular formula:C12H30Si2
- Molecular Weight:230.54
617-86-7
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Yield: 80%
Reaction Conditions:
with silver carbonate in methanol at 60; for 14 h;
Steps:
6 Example 7 The reaction formula of this embodiment is as follows:
Ag2CO3 (0.0125 mmol, 0.0034 g) was added to the reaction flask, methanol (MeOH, 2.5 ml) was added, and 1 mmol (0.2907 g) of 2.5 mmol of the compound was slowly added dropwise to the reaction flask. The reaction was stirred at 60 ° C for 12 After 2 hours, 2 g (0.24335 g) of the product was obtained by distillation under reduced pressure after the reaction was completed, and the yield was 80%.
References:
Xuzhou Medical University;Wu Nan;Li Chuang;Mi Jiajia;Zheng Yan;Yu Ruobing;Yuan Changyong;Xu Zhou CN110669066, 2020, A Location in patent:Paragraph 0058-0061
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![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
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