m-Toluic acid synthesis
- Product Name:m-Toluic acid
- CAS Number:99-04-7
- Molecular formula:C8H8O2
- Molecular Weight:136.15
620-22-4
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$14.00/25mL
99-04-7
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$8.00/100g
Yield:99-04-7 98.5%
Reaction Conditions:
with water;sodium hydroxide at 100; for 4 h;Temperature;
Steps:
1-3
To 2000ml with mechanical stirring, thermometer, reflux condenser, add 117g of m-toluonitrile, 800g of water, and 200g of sodium hydroxide solution with a mass fraction of 30% to the four-neck flask of the heating device, and start stirring. The temperature was raised to 100 °C and the reaction was carried out under reflux for 4h. Then, hydrochloric acid with a mass fraction of 30% was added dropwise to adjust the pH to 1. After cooling to room temperature, it was filtered, washed with water, filter and dry to get 134g m-toluic acid, the reaction yield at this step was 98.5%.
References:
CN110981719,2020,A Location in patent:Paragraph 0040-0041; 0045-0046; 0050-0051
53663-39-1
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$8.00/1g
99-04-7
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$8.00/100g
620-23-5
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$5.00/5g
99-04-7
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$8.00/100g
587-03-1
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$21.00/5g
99-04-7
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$8.00/100g
7287-81-2
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$45.00/25mg
99-04-7
475 suppliers
$8.00/100g