methyl 7-oxoheptanoate synthesis
- Product Name:methyl 7-oxoheptanoate
- CAS Number:35376-00-2
- Molecular formula:C8H14O3
- Molecular Weight:158.2
6089-09-4
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35376-00-2
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$509.56/5MG
Yield:-
Steps:
Multi-step reaction with 9 steps
1.1: 96 percent / potassium carbonate / dimethylformamide / 20 °C
2.1: potassium carbonate; CuCl; Bu4NI / dimethylformamide / 0.17 h / 20 °C
2.2: dimethylformamide
3.1: 8.3 g / OsO4; N-methylmorpholine N-oxide / H2O; tetrahydrofuran; acetone / 10 h / 20 °C
4.1: 97 percent / hydrogen / Lindlar catalyst / ethyl acetate / 4 h
5.1: 82 percent / p-TsOH / acetone / 2 h / 20 °C
6.1: 97 percent / hydrogen / Pd/C / ethyl acetate / 3 h
7.1: 80 percent / DCC; 4-(dimethylamino)pyridine / CH2Cl2 / 3 h / 20 °C
8.1: 77 percent / p-TsOH / methanol / 4 h / 20 °C
9.1: 78 percent / aq. NaIO4 / CH2Cl2 / 0.33 h / 20 °C
References:
Wen, Shijun;Carey, Krystle L.;Nakao, Yoichi;Fusetani, Nobuhiro;Packham, Graham;Ganesan [Organic Letters,2007,vol. 9,# 6,p. 1105 - 1108]
14565-11-8
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35376-00-2
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67-56-1
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628-92-2
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35444-47-4
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13154-41-1
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35376-00-2
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