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Methylprednisolone aceponate synthesis

2synthesis methods

Yield:-

Steps:

Multi-step reaction with 2 steps
1: 2 N aq. oxalic acid / methanol / 0.17 h / 40 - 45 °C
2: Et₃N / CH₂Cl₂ / 3 h / Ambient temperature

References:

Sugai;Okazaki;Kajiwara;Kanbara;Naito;Yoshida;Akaboshi;Ikegami;Kamano [Chemical and Pharmaceutical Bulletin,1985,vol. 33,# 5,p. 1889 - 1898]

Prednisolone-21-acetate Methylprednisolone acetate Prednisolone Prednisone 2,2-Bis(hydroxymethyl)propionic acid Meprednisone Deprodone

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