MPT0E028 synthesis
- Product Name:MPT0E028
- CAS Number:1338320-94-7
- Molecular formula:C17H16N2O4S
- Molecular Weight:344.38
1011-65-0
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Yield:-
Steps:
Multi-step reaction with 8 steps
1.1: sodium cyanoborohydride; acetic acid / 2 h / 0 - 20 °C
1.2: 0 °C / pH 10
2.1: pyridine / Reflux
3.1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 - 20 °C
4.1: dipyridinium dichromate / dichloromethane / 20 °C / Molecular sieve
5.1: dichloromethane / 3 h / 20 °C
6.1: water; lithium hydroxide / 1,4-dioxane / 40 °C
7.1: triethylamine; benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate / N,N-dimethyl-formamide / 1 h / 20 °C
8.1: trifluoroacetic acid / methanol / 20 °C
References:
US2011/245315,2011,A1
141452-01-9
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1241118-90-0
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