N-ALLYL-N-METHYLANILINE synthesis
- Product Name:N-ALLYL-N-METHYLANILINE
- CAS Number:6628-07-5
- Molecular formula:C10H13N
- Molecular Weight:147.22
71492-76-7
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Yield:6628-07-5 100%
Reaction Conditions:
Stage #1: N-allyl-N-methyl-2-bromoanilinewith tert.-butyl lithium in diethyl ether;pentane at -78; for 1 h;
Stage #2: with indium(III) chloride in tetrahydrofuran;diethyl ether;pentane at -78; for 1 h;
Stage #3: with water in tetrahydrofuran;diethyl ether;pentane;Heating;Further stages.;
References:
Hirashita, Tsunehisa;Hayashi, Ayumi;Tsuji, Makoto;Tanaka, Jiro;Araki, Shuki [Tetrahedron,2008,vol. 64,# 11,p. 2642 - 2650]
