N-HEXYLTRIMETHOXYSILANE synthesis
- Product Name:N-HEXYLTRIMETHOXYSILANE
- CAS Number:3069-19-0
- Molecular formula:C9H22O3Si
- Molecular Weight:206.35
592-41-6
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2487-90-3
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$130.00/5g
3069-19-0
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$7.00/5g
Yield:3069-19-0 100%
Reaction Conditions:
at 90; for 5 h;Inert atmosphere;
Steps:
17 Example 17
In a 500-ml three-necked flask, hexene (1.25 mol) was added, and Catalyst 1 (1.25 mmol) prepared in Example 1 was slowly heated to 90°C under nitrogen protection.While stirring, trimethoxyhydrosilane (1.5 mol) was added dropwise via a dropping funnel. The dropwise addition time was 0.5 hours. The reaction temperature was maintained and the reaction was continued for 5 hours.After cooling to room temperature, the corresponding fraction was collected by distillation under reduced pressure, and the conversion of hexene was determined by GC-MS to be 89.0%.The yield of the β adduct 1-trimethoxysilylhexane was 100%.
References:
CN107857776,2018,A Location in patent:Paragraph 0060; 0061
681-84-5
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$27.09/25g
3069-19-0
166 suppliers
$7.00/5g