N-Methylbenzylamine synthesis
- Product Name:N-Methylbenzylamine
- CAS Number:103-67-3
- Molecular formula:C8H11N
- Molecular Weight:121.18
25521-74-8
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Yield:103-67-3 99%
Reaction Conditions:
with palladium 10% on activated carbon;hydrogen in dichloromethane at 20; under 760.051 Torr; for 3 h;
Steps:
ENTRY 22. Reduction of (E)-N-methyl-1-phenylmethanimine to N-benzylmethylamine.
A mixture of (E)-N-methyl-1-phenylmethanimine (359 mg, 3.01 mmol) and 10% palladium on carbon (160 mg) in DCM (30 mL) was vigorously stirred under hydrogen for 3 h.
References:
Mason, David J.;Timofeyenko, Yegor G.;Jagadish, Bhumasamudram;Mash, Eugene A. [Synthetic Communications,2022,vol. 52,# 18,p. 1825 - 1833] Location in patent:supporting information
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103-67-3
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103-67-3
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103-67-3
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