N-METHYLDIHEXYLAMINE synthesis
- Product Name:N-METHYLDIHEXYLAMINE
- CAS Number:37615-53-5
- Molecular formula:C13H29N
- Molecular Weight:199.38
100799-35-7
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Yield: 90%
Reaction Conditions:
with phenylboronic acid in 1,2-dichloro-ethane at 80; for 0.75 h;
Steps:
Deoxygenation of aliphatic and heteroaromatic amine N-oxides
General procedure: Phenylboronic acid (1.0 equiv. for aliphatic N-oxides and 1.5 equiv. for pyridine N-oxides) and tert-amine N-oxide (1 mmol) was stirred in dichloroethane (2 mL) at appropriate temperature (80 oC and 120 oC respectively) in a pressure tube. The progress of the reaction was monitoredby using TLC. After completion, the reaction mixture was diluted with ethyl acetate and washed with water and NaOH solution (1 normal, 3*5 mL). The organic layer was dried over anhydrous sodium sulfate, evaporated and subjected to the column chromatography to obtain pure products.
References:
Gupta, Surabhi;Sureshbabu, Popuri;Singh, Adesh Kumar;Sabiah, Shahulhameed;Kandasamy, Jeyakumar [Tetrahedron Letters,2017,vol. 58,# 10,p. 909 - 913] Location in patent:supporting information
![Ethanamine, N-[(3,5-dichlorophenyl)methylene]-2,2-diethoxy-](/CAS/20210305/GIF/1000210-73-0.gif)
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37615-53-5
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4385-04-0
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37615-53-5
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35161-70-7
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4385-04-0
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37615-53-5
23 suppliers
$68.90/5ml