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ChemicalBook CAS DataBase List N-NONANE
111-84-2

N-NONANE synthesis

12synthesis methods
-

Yield:111-84-2 9% ,629-78-7 90.6%

Reaction Conditions:

with C31H37ClN3NiO2(1-)*Li(1+) in tetrahydrofuran at 25; for 0.333333 h;Inert atmosphere;Overall yield = 99.6 %;

Steps:

2.5 Cross coupling of CHCl3 and CCl4 with Grignard reagent

General procedure: Cross-coupling reactions of Grignard reagents with CHCl3 and CCl4 were performed according to the following general method. Catalyst 2 (1 mg, 1.74 μmol) in 1 mL THF was added using a gas-tight syringe to a 5 mL round bottom flask purged with N2. To this solution 2 M n-butylmagnesium chloride in THF (0.63 mL, 1.26 mmol) was added. CHCl3 (34 μL, 0.42 mmol) was added to the reaction mixture. In the case of reactions with CCl4 (40 μL, 0.42 mmol), 1.68 mmol of Grignard reagent was added. Samples were collected for analysis after 20 min. At the end of the reaction, excess Grignard reagent was destroyed using methanol and the reaction products were analyzed by GC-MS using an internal standard to quantify product formation.

References:

Gartia, Yashraj;Nasini, Udaya Bhasker;Ghosh, Anindya;Biswas, Abhijit;Stadler, Matthew [Journal of Molecular Catalysis A: Chemical,2012,vol. 363-364,p. 322 - 327,6]

N-NONANE Related Search:

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