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ChemicalBook CAS DataBase List Octadecane
593-45-3

Octadecane synthesis

14synthesis methods
-

Yield:593-45-3 96%

Reaction Conditions:

with palladium 10% on activated carbon;hydrogen in dichloromethane at 20; under 760.051 Torr; for 12 h;

Steps:

ENTRY 2. Reduction of 1-octadecyne to octadecane.

A mixture of 1-octadecyne (750 mg, 2.99 mmol) and 10% palladium on carbon (162 mg) in DCM (30 mL) was vigorously stirred under hydrogen for 12 h.

References:

Mason, David J.;Timofeyenko, Yegor G.;Jagadish, Bhumasamudram;Mash, Eugene A. [Synthetic Communications,2022,vol. 52,# 18,p. 1825 - 1833] Location in patent:supporting information

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