Nitrosobenzene synthesis
- Product Name:Nitrosobenzene
- CAS Number:586-96-9
- Molecular formula:C6H5NO
- Molecular Weight:107.11
62-53-3
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586-96-9
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Yield:586-96-9 90%
Reaction Conditions:
with urea hydrogen peroxide adduct;carbonic acid dimethyl ester at 20; for 2 h;Catalytic behavior;Reagent/catalyst;Temperature;
Steps:
General procedure for amine oxidation to nitrosoarene
General procedure: To a solution of 1 mmol amine in 2 mL DMC, was added3 mmol UHP and 0.03 g catalyst. The mixture was stirredat room temperature for 2 h. Then the catalyst was removedusing magnetic decantation. The reaction vessel was washedwith water and extracted with dichloromethane (3 × 10 mL).The organic layer was dried with Na2SO4and the solventwas evaporated under vacuum. The crude product was purifiedusing column chromatography if needed.
References:
Jadidi Nejad, Masoume;Yazdani, Elahe;Kazemi Miraki, Maryam;Heydari, Akbar [Chemical Papers,2019,vol. 73,# 7,p. 1575 - 1583]
98-95-3
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62-53-3
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$10.00/1g
586-96-9
130 suppliers
$20.00/1G
495-48-7
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$36.29/10g
62-53-3
682 suppliers
$10.00/1g
98-95-3
38 suppliers
$14.00/25g
586-96-9
130 suppliers
$20.00/1G
1227476-15-4
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100-65-2
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586-96-9
130 suppliers
$20.00/1G