pentyl (2,4-dichlorophenoxy)acetate synthesis
- Product Name:pentyl (2,4-dichlorophenoxy)acetate
- CAS Number:1917-92-6
- Molecular formula:C13H16Cl2O3
- Molecular Weight:291.17
74525-52-3
3 suppliers
inquiry
1917-92-6
2 suppliers
inquiry
Yield:1917-92-6 290.54 g
Reaction Conditions:
with 2-ethylthiazole;chlorine;titanium(IV) oxide at 50; for 0.5 h;
Steps:
7
1.27 g of 99% titanium dioxide was added to n-pentyl phenoxyacetate.0.58 g of 99% 2-ethylthiazole was reacted at 151.34 g of 99% chlorine gas at 50 ° C, and the reaction was kept at this temperature for 0.5 h.Distilling and collecting fractions at 135-145 ° C under a pressure of 1 kpa,2,4-dichlorophenoxyacetic acid n-amyl ester 290.54g,The content is 99.08%.
References:
CN108947838,2018,A Location in patent:Paragraph 0111; 0113
71-41-0
456 suppliers
$10.00/25mL
1917-92-6
2 suppliers
inquiry