S-ATBA synthesis
- Product Name:S-ATBA
- CAS Number:109010-60-8
- Molecular formula:C16H22N2O3
- Molecular Weight:290.36
![3-Bromo-1,3,4,5-tetrahydro-2H-benzo[b]azepin-2-one](/CAS/GIF/86499-96-9.gif)
86499-96-9
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109010-60-8
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Yield:-
Steps:
Multi-step reaction with 3 steps
1: 93 percent / Na2CO3, propylene glycol / 3.5 h / 130 °C
2: 88 percent / odorless mineral spirits / 16 h / 140 °C
3: 1.) tetrabutylammonium hydrogen sulfate, 50percent NaOH, 3.) H2 / 3.) 5percent Pd/C / 1.) toluene, 35 deg C, 1 h; 20 deg C, 16 h, 2.) toluene, 20 deg C, 1 h, 3.) EtOH, 60 deg C, 55 psi, 16 h
References:
Shieh;Carlson;Zaunius [Journal of Organic Chemistry,1997,vol. 62,# 23,p. 8271 - 8272]
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197658-51-8
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109010-60-8
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107-59-5
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![[S-(R*,R*)]-1,3,4,5-Tetrahydro-3-[(1-phenylethyl)amino]-2H-1-benzazepin-2-one](/CAS/20150408/GIF/197658-50-7.gif)
197658-50-7
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109010-60-8
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529-23-7
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109010-60-8
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