Sodium triacetoxyborohydride synthesis
- Product Name:Sodium triacetoxyborohydride
- CAS Number:56553-60-7
- Molecular formula:C6H10BNaO6
- Molecular Weight:211.94
64-19-7
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56553-60-7
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Yield:-
Reaction Conditions:
with sodium tetrahydroborate in 2-methylpropyl acetate at 0 - 5; for 1 h;
Steps:
2
The sodium triacetoxyborohydride suspension was prepared as follows: to a suspension of 6.5 g (~170 mmol) of sodium borohydride in 125 mL of isobutyl acetate, 21.55 mL (22.6 g, 376 mmol) of acetic acid was added dropwise while the temperature was kept between 0-50C. The obtained white suspension was then stirred below 50C for about one hour before being used.
References:
WO2008/68625,2008,A2 Location in patent:Page/Page column 19
16940-66-2
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64-19-7
1726 suppliers
$10.00/25ML
56553-60-7
635 suppliers
$10.00/5g
16940-66-2
0 suppliers
$21.21/100ml
56553-60-7
635 suppliers
$10.00/5g