trans-2-Hexenoic acid synthesis
- Product Name:trans-2-Hexenoic acid
- CAS Number:13419-69-7
- Molecular formula:C6H10O2
- Molecular Weight:114.14
6728-26-3
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13419-69-7
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Yield:13419-69-7 99%
Reaction Conditions:
with diphenyl diselenide;dihydrogen peroxide in water at 20; for 6 h;Green chemistry;
Steps:
3.2. General Procedure for the Synthesis of Carboxylic Acids 2
General procedure: Diphenyl diselenide (3, 0.006 g; 0.02 mmol) was treated with H2O2 (30%·w/w, 0.1 mL, 1 mmol) andwater (0.2 mL) and stirred at room temperature at 800 rpm until the discoloration of the reaction mixture;then, the aldehyde 1 (1 mmol) was added. After 6 h, the aqueous mixture was extracted three times withEtOAc (3 × 20 mL). The collected organic layers were dried over Na2SO4 and the solvent evaporatedunder reduced pressure.
References:
Sancineto, Luca;Tidei, Caterina;Bagnoli, Luana;Marini, Francesca;Lenardo, Eder J.;Santi, Claudio [Molecules,2015,vol. 20,# 6,p. 10496 - 10510]
85144-28-1
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13419-69-7
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141-82-2
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123-72-8
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13419-69-7
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3095-95-2
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123-72-8
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13419-69-7
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27829-72-7
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13419-69-7
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