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ChemicalBook CAS DataBase List Trifluoromethanesulfonamide
421-85-2

Trifluoromethanesulfonamide synthesis

9synthesis methods
15.39 trifluoromethanesulfonyl chloride dissolved in 103 g of anhydrous isopropyl ether is charged to a reactor. The medium is cooled to 5 °C. and the ammonia is added slowly over 2 hours. After 5 hours of stirring at 5° C., 24.8 g of water are added to dissolve the salts. The medium is then acidified by adding 20.7 g of a 36% aqueous hydrochloric acid solution.   
After a further addition of 13 g of water, the phases are separated. The aqueous phase is washed with 50 g of isopropyl ether. The organic phases are combined and the solvent is removed under reduced pressure.
10.15 g of a white solid of trifluoromethanesulfonamide are thus obtained.
-

Yield:421-85-2 96%

Steps:

1 Step 1:

Step 1: Trifluoromethylsulphonamide : The title compound was prepared using the same procedure as described in Example 12, Step 1, replacing isopropylsulphonyl chloride with trifluoromethylsulphonyl chloride. The compound was purified by trituration with hexane to give the product (8.5g, 96%) as a colourless solid. mp 116-119°C.

References:

EP514133,1992,A1

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